Patent
A method for preparing a solid electrolyte
Liu Fangyang,Lai Yanqing,Sun Zhen,Xu Xiangqun,Jiang Liangxing,Jia Ming,Li Jie,Liu Yexiang +7 more
- 21 Dec 2018
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TL;DR: In this paper, a method for preparing a solid electrolyte comprises weighing lithium salt, zirconium salt and phosphate according to a required stoichiometric ratio and uniformly mixing the same.
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Abstract: A method for preparing a solid electrolyte comprises weighing lithium salt, zirconium salt and phosphate according to a required stoichiometric ratio and uniformly mixing the same; (2) pre-burning theuniformly mixed the mixture in microwave at 400 to 800 degree centigrade for 2 to 6 hours; (3) grinding the pre-burned mixture evenly and pressing into tablets, and then pressing the tablets in microwave at 800 to 1000 degree centigrade for 2 to 6 hours, and obtaining a LiZr2 (PO4) 3 solid electrolyte. Compared with the prior art, the sintering temperature of the invention is low, the productioncycle is short, the rhombus structure LiZr2 (PO4) 3 which is stable at room temperature can be obtained, and the ionic conductivity of the rhombus structure LiZr2 (PO4) 3 reaches 1.0 * 10-6 ~ 8.0 * 10-5S/cm.
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Citations
Patent
Halide solid electrolyte, preparation method thereof and lithium ion battery
Yang Dunjie
- 10 Apr 2020
TL;DR: In this paper, a halide solid electrolyte, a preparation method thereof and a lithium ion battery are provided, which is based on a ball-milling of lithium halide and non-metal halide to obtain a mixture.
1
References
Patent
Solid electrolyte separator bonding agent
Zhebo Chen,Niall Donnelly,Tim Holme,Deepika Singh +3 more
- 15 May 2017
TL;DR: In this article, the authors present electrochemical cells which include a negative electrode current collector, a lithium metal negative electrode, an oxide electrolyte membrane, a bonding agent layer, a positive electrode, and a positive current collector.
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Divalent alkaline-earth metal and tantalum co-doped Li7La3Zr2O12 solid electrolyte material and preparation method
Zhao Hailei,Xu Tao,Zhang Saisai +2 more
- 12 Jun 2018
TL;DR: In this article, a divalent alkaline-earth metal and tantalum co-doped Li7La3Zr2O12 electrolyte material and a preparation method, which belongs to the field of electrolyte materials.
7
Patent
Method for preparing composite solid electrolyte
Yang Xing,Liu Xiaoyan,Wang Haitao +2 more
- 24 Nov 2017
TL;DR: In this article, a method for preparing composite solid electrolyte is presented, which comprises the following steps: I, dissolving a polyoxyethylene monomer into an organic solvent, stirring at a certain temperature, and filtering so as to obtain a high-molecular polymer; II, adding Ru(Cp*)Cl(PPh3)2 into the highmolescular polymer, and the polyoxy methylene monomers of the step I dissolving into an O(PEO-PST two-phase polymer; III, performing uniform-ball-m
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Patent
Preparation method of titanium phosphate/germanium-aluminum-lithium solid electrolyte
Ding Fei,Xu Zhibin,Zhong Hai,Jianyu Liu,Zhiyuan Tang +4 more
- 20 Oct 2017
Abstract: The invention relates to a preparation method of a titanium phosphate/germanium-aluminum-lithium solid electrolyte, and belongs to the technical field of solid electrolytes. The preparation method of the titanium phosphate/germanium-aluminum-lithium solid electrolyte is characterized by adopting a molten salt assisted solid phase method, enabling fused salt to become a molten state so as to provide a liquid state environment beneficial to fully mixing a precursor, and obtaining a solid electrolyte material with the characteristics that Li1+xAlxM2-x(PO4)3x is equal to 0 to 0.7 and M is equal to Ti and Ge. The preparation method of the titanium phosphate/germanium-aluminum-lithium solid electrolyte provided by the invention has the advantages of simple production process, convenience in industrial production, high ionic conductivity of the product solid electrolyte material at the room temperature, stable product quality and the like.
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Patent
Method for manufacturing lithium ion conductive solid electrolyte thin film
Kazunori Takada,Shigeo Kondo,Watanabe Jun,Kenjiro Fujimoto,Taro Inada,Akihisa Kajiyama,Takaguchi Masaru +6 more
- 12 Apr 2002
TL;DR: In this paper, a method for manufacturing a lithium ion conducting solid electrolyte thin film, a solution containing phosphoric ester expressed by at least alkoxide of lithium and alkoxide ion of titanium, PO(OH)3-x(OR)x (OR is alkoxyl group, 0
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