One‐dimensional (1D) nanostructured photocatalyst is a promising candidate for hydrogen (H2) generation, which can be used to deal with the energy crisis. Herein, novel 1D TiO2/CdS well‐hybridized nanofibers (NFs) were synthesized via in situ electrospinning method. These 1D hybrid NFs showed a high H2‐production rate of 2.32 mmol h−1 g−1 with an apparent quantum efficiency of 10.14 %, which was 35‐fold higher than that of pristine TiO2 NFs. X‐ray photoelectron spectroscopy (XPS) analysis and density functional theory calculation implied that the electrons transferred from CdS to TiO2 upon hybridization and created an internal electric field (IEF) pointing from CdS to TiO2. This IEF drove the photoexcited electrons in TiO2 to transfer toward CdS upon light irradiation as revealed by in situ irradiated XPS analysis, suggesting that a step‐scheme (S‐scheme) heterojunction was formed in the TiO2/CdS nanohybrids and greatly promoted the separation of electron‐hole pairs to foster efficient H2 photogeneration. The significant enhancement of photocatalytic activity was also benefited from the easy transfer for electrons in the 1D well‐distributed nanostructure of nanohybrids. This work presents a method for in situ preparing well‐distributed 1D NFs with high photocatalytic activity for H2 production via the S‐scheme pathways.

S‐Scheme Heterojunction TiO2/CdS Nanocomposite Nanofiber as H2‐Production Photocatalyst

BiVO4, Bi2WO6 and Bi2MoO6 photocatalysis: A brief review

One-pot solvothermal fabrication of S-scheme OVs-Bi2O3/Bi2SiO5 microsphere heterojunctions with enhanced photocatalytic performance toward decontamination of organic pollutants

https://www.cjcatal.com/EN/article/downloadArticleFile.do?attachType=PDF&id=26306

2D metal-free heterostructure of covalent triazine framework/g-C3N4 for enhanced photocatalytic CO2 reduction with high selectivity

Pharmaceuticals have been classified as emerging water pollutants which are recalcitrant in nature. In the quest to find a suitable technique in removing them from contaminated water, photoelectrocatalytic oxidation method has attracted much attention in recent years. This report examined the feasibility of degrading ciprofloxacin and sulfamethoxazole through photoelectrocatalytic oxidation using FTO-BiVO4/Ag2S with p-n heterojunction as anode. BiVO4/Ag2S was prepared through electrodeposition and successive ionic layer adsorption/reaction on FTO glass. Structural and morphological studies using XRD, SEM, EDS and diffusive reflectance UV-Vis confirmed the successful construction of p-n heterojunction of BiVO4/Ag2S. Electrochemical techniques were used to investigate enhanced charge separation in the binary electrode. The FTO-BiVO4/Ag2S electrode exhibited the highest photocurrent response (1.194 mA/cm−2) and longest electron lifetime (0.40 ms) than both pristine BiVO4 and Ag2S electrodes which confirmed the reduction in recombination of charge carriers in the electrode. Upon application of the prepared FTO-BiVO4/Ag2S in photoelectrocatalytic removal of ciprofloxacin and sulfamethoxazole, percentage removal of 80% and 86% were achieved respectively with a low bias potential of 1.2 V (vs Ag/AgCl) within 120 min. The electrode possesses good stability and reusability. The results obtained revealed BiVO4/Ag2S as a suitable photoanode for removing recalcitrant pharmaceutical molecules in water.

Towards visible light driven photoelectrocatalysis for water treatment: Application of a FTO/BiVO 4 /Ag 2 S heterojunction anode for the removal of emerging pharmaceutical pollutants

Enhancement mechanism of fiddlehead-shaped TiO2-BiVO4 type II heterojunction in SPEC towards RhB degradation and detoxification

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Enhancement mechanism of fiddlehead-shaped TiO2-BiVO4 type II heterojunction in SPEC towards RhB degradation and detoxification