High-temperature measurements above 1000 °C are critical in harsh environments such as aerospace, metallurgy, fossil fuel, and power production. Fiber-optic high-temperature sensors are gradually replacing traditional electronic sensors due to their small size, resistance to electromagnetic interference, remote detection, multiplexing, and distributed measurement advantages. This paper reviews the sensing principle, structural design, and temperature measurement performance of fiber-optic high-temperature sensors, as well as recent significant progress in the transition of sensing solutions from glass to crystal fiber. Finally, future prospects and challenges in developing fiber-optic high-temperature sensors are also discussed.

/pdf/optical-fiber-sensors-for-high-temperature-monitoring-a-152krzok.pdf

Optical Fiber Sensors for High-Temperature Monitoring: A Review

The current generation is witnessing a huge interest in optical waveguides due to their salient features: they are of low cost, immune to electromagnetic interference, easy to multiplex, have a compact size, etc. These features of optical fibers make them a useful tool for various sensing applications including in medicine, automotives, biotechnology, food quality control, aerospace, physical and chemical monitoring. Among all the reported applications, optical waveguides have been widely exploited to measure the physical and chemical variations in the surrounding environment. Optical fiber-based temperature sensors have played a crucial role in this decade to detect high fever and tackle COVID-19-like pandemics. Recognizing the major developments in the field of optical fibers, this article provides recent progress in temperature sensors utilizing several sensing configurations including conventional fiber, photonic crystal fiber, and Bragg grating fibers. Additionally, this article also highlights the advantages, limitations, and future possibilities in this area.

/pdf/optical-fiber-based-temperature-sensors-a-review-2fmxnyp3.pdf

Optical Fiber Based Temperature Sensors: A Review

This paper presents a comprehensive review of optical fiber sensors (OFSs), including FBG, distributed optical fiber sensor and Fabry-Perot interferometer, and their applications within harsh environments, which include extremely high temperatures (from 275 °C to 1750 °C) and low temperatures (from −271.15 °C to −40 °C, namely cryogenic conditions: from 2 K to 233.15 K), and high levels of ionizing radiation (with a maximum gamma dose up to 2 GGy, and a maximum neutron fluence of approximately $5 \times 10^{19}$ n/cm2). After a brief introduction of the principles of OFSs and mechanisms of interrogation, this paper focuses on the existing works for the above three operating environments. Attention have been paid to material selection for fabricating fibers, effects of doping with rare earth elements, femtosecond laser engraving, pre-processing and post-processing (i.e., annealing) that are employed to overcome issues faced byOFSs in extreme temperatures and radiation environments. Application examples and practical test cases are also presented. Through these examples, the limitations in the current state-of-the-art are acknowledged and the key problems are identified. Potential solutions to some of these problems are also elucidated. A feature of this paper is the amalgamation of many research methodologies and outcomes in three seemingly distinct environmental conditions in one place so that different solution techniques can be integrated to advance OFS technologies, especially for extreme environment applications.

Optical Fiber Sensors in Extreme Temperature and Radiation Environments: A Review

In situ measurement of high temperature is critical in aerospace, petrochemical, metallurgical, and power industries. The single-crystal sapphire fiber is a promising material for high-temperature measurement owing to its high melting point of ∼2045 °C. Sapphire fiber Bragg gratings (SFBGs), which could be inscribed in sapphire fibers with a femtosecond laser, are widely used as high-temperature sensors. However, conventional SFBGs typically exhibit a significant deterioration in their spectra after long-term operation at ultra-high temperatures, resulting from the formation of some unwanted microstructural features, that is, lossy spots and micro-etched lines, on the surface of the sapphire fiber. Here, we report for the first time, to the best of our knowledge, a thermally stabilized ultra-high-temperature sensor based on an SFBG created by femtosecond laser inscription, inert gas-sealed packaging, and gradient temperature-elevated annealing. The results indicate that the lossy spots are essentially aluminum hydroxide induced by high-temperature oxidation, and the inert gas-sealed packaging process can effectively insulate the sapphire fiber from the ambient air. Moreover, the formation of micro-etched lines was suppressed successfully by using the gradient temperature-elevated annealing process. As a result, the surface topography of the SFBG after operating at high temperatures was improved obviously. The long-term thermal stability of such an SFBG was greatly enhanced, showing a stable operation at 1600 °C for up to 20 h. In addition, it could withstand an even higher temperature of 1800 °C with a sensitivity of 41.2 pm/°C. The aforementioned results make it promising for high-temperature sensing in chemical, aviation, smelting, and power industries.

Stabilized Ultra-High-Temperature Sensors Based on Inert Gas-Sealed Sapphire Fiber Bragg Gratings.

Sapphire optical fiber has the ability to withstand ultrahigh temperatures and high radiation, but it is multimoded which prevents its use in many sensing applications. Problematically, Bragg gratings in such fiber exhibit multiple reflection peaks with a fluctuating power distribution. In this work, we write single-mode waveguides with Bragg gratings in sapphire using a novel multi-layer depressed cladding design in the 1550 nm telecommunications waveband. The Bragg gratings have a narrow bandwidth (<0.5 nm) and have survived annealing at 1000°C. The structures are inscribed with femtosecond laser direct writing, using adaptive beam shaping with a non-immersion objective. A single-mode sapphire fiber Bragg grating is created by writing a waveguide with a Bragg grating within a 425 µm diameter sapphire optical fiber, providing significant potential for accurate remote sensing in ultra-extreme environments. 

/pdf/single-mode-sapphire-fiber-bragg-grating-3r2zkfxu.pdf

Single-mode sapphire fiber Bragg grating

Ultra-weak fiber Bragg grating (UWFBG) arrays are key elements for constructing large-scale quasi-distributed sensing networks for structural health monitoring. Conventional methods for creating UWFBG arrays are based on in-line UV exposure during fiber drawing. However, the UV-induced UWFBG arrays cannot withstand a high temperature above 450 °C. Here, we report for the first time, to the best of our knowledge, a new method for fabricating high-temperature-resistant UWFBG arrays by using a femtosecond laser point-by-point (PbP) technology. UWFBGs with a low peak reflectivity of ∼ - 45 dB (corresponding to ∼ 0.0032%) were successfully fabricated in a conventional single-mode fiber (SMF) by femtosecond laser PbP inscription through fiber coating. Moreover, the influences of grating length, laser pulse energy, and grating order on the UWFBGs were studied, and a grating length of 1 mm, a pulse energy of 29.2 nJ, and a grating order of 120 were used for fabricating the UWFBGs. And then, a long-term high-temperature annealing was carried out, and the results show that the UWFBGs can withstand a high temperature of 1000 °C and have an excellent thermal repeatability with a sensitivity of 18.2 pm/°C at 1000 °C. A UWFBG array consisting of 200 identical UWFBGs was successfully fabricated along a 2 m-long conventional SMF with an interval of 10 mm, and interrogated with an optical frequency domain reflectometer (OFDR). Distributed high-temperature sensing up to 1000 °C was demonstrated by using the fabricated UWFBG array and OFDR demodulation. As such, the proposed femtosecond laser-inscribed UWFBG array is promising for distributed high-temperature sensing in hash environments, such as aerospace vehicles, nuclear plants, and smelting furnaces.

Femtosecond laser point-by-point inscription of an ultra-weak fiber Bragg grating array for distributed high-temperature sensing.

Sapphire fiber Bragg gratings (SFBGs) inscribed by using femtosecond laser point-by-point (PbP) technology typically have an extremely low reflectivity due to the limited cross-sectional area of refractive index modulations (RIMs) created in sapphire fiber. Hence, we propose and experimentally demonstrate a filamentation process for fabricating PbP SFBGs. This approach provides an efficient method for producing SFBGs at various Bragg wavelengths with a higher reflectivity, since the filament tracks could enlarge the cross-sectional area of RIMs. The influences of the pulse energy and the focal depth on the generation and morphology of the filament tracks were studied, and after optimizing these parameters, high-quality filament tracks with a length of 90 µm and a width of 1.4 µm were produced into sapphire fiber with a diameter of 100 µm. These filament tracks were precisely assembled in sapphire fiber, generating an SFBG with a reflectivity of 2.3%. The total fabrication time for this SFBG only requires ${\sim}{1.1}\;{\rm s}$. Subsequently, a wavelength-division-multiplexed (WDM) SFBG array consisting of five SFBGs was efficiently constructed. Moreover, the high-temperature response of the SFBG array was investigated and the experimental results showed that the SFBG array can withstand a high temperature of 1600°C. Such a WDM SFBG array could serve as quasi-distributed high-temperature sensor which will be promising in many areas, i.e., metallurgical, chemical, and aviation industries.

Efficient point-by-point Bragg grating inscription in sapphire fiber using femtosecond laser filaments

We demonstrate the fabrication of single-mode helical Bragg grating waveguides (HBGWs) in a multimode coreless fiber by using a femtosecond laser direct writing technique. This approach provides a single-step method for creating Bragg grating waveguides. Specifically, the unique helical structure in such an HBGW serves as a depressed cladding waveguide and also generates strong Bragg resonance due to its periodicity. Effects of pulse energy, helical diameter, and helical pitch used for fabricating HBGWs were studied, and a single-mode HBGW with a narrow bandwidth of 0.43 nm and a Bragg wavelength of 1546.50 nm was achieved by using appropriate parameters, including a diameter of 10 μm and a helical pitch of 1.07 μm. The measured cross-sectional refractive index profile indicates that a depressed cladding waveguide has been created in this single-mode HBGW. Moreover, five single-mode HBGWs with various Bragg wavelengths were successfully fabricated by controlling the helical pitch, and this technique could be used for achieving a wavelength-division-multiplexed HBGW array. Then, the temperature and strain responses of the fabricated single-mode HBGW were tested, exhibiting a temperature sensitivity of 11.65 pm/°C and a strain sensitivity of 1.29 pm/μe, respectively. In addition, the thermal stability of the single-mode HBGW was also studied by annealing at a high temperature of 700°C for 15 h. The degeneration of the single-mode waveguide into a multimode waveguide was observed during the isothermal annealing process, and the peak reflection and the Bragg wavelength of the fundamental mode exhibited a decrease of ∼7  dB and a “blue” shift of 0.36 nm. Hence, such a femtosecond laser directly written single-mode HBGW could be used in many applications, such as sapphire fiber sensors, photonic integrated circuits, and monolithic waveguide lasers.

/pdf/single-mode-helical-bragg-grating-waveguide-created-in-a-55dfgnvukt.pdf

Single-mode helical Bragg grating waveguide created in a multimode coreless fiber by femtosecond laser direct writing

Fiber Bragg gratings (FBGs) inscribed by using femtosecond laser point-by-point (PbP) technology typically have high birefringence due to the elliptical cross-sectional pattern of refractive index modulations (RIMs) created in the fiber core. Additionally, a highly reflective type II PbP FBG, which has a large coupling coefficient, also exhibits large insertion loss due to the limited RIM area induced by a single femtosecond laser pulse. Here we demonstrate a slit beam shaping method for femtosecond laser PbP inscription of high-quality FBGs, featuring by high reflectivity, low insertion loss, and low birefringence. The slit beam shaping method could reduce the ellipticity in the cross-sectional pattern of RIMs without reducing the cross-sectional area, leading to low birefringence and low insertion loss. The experimental results agree well with numerical calculations. Hence, a high-quality type II PbP FBG, which has high reflectivity of 99.12% (i.e., Bragg resonance attenuation of 20.52 dB), low insertion loss of 0.30 dB, and low birefringence of 1.86 × 10−6, was successfully created by use of a slit width of 0.8 mm. Moreover, an enlarged cross-sectional area was created by use of a slit width of 0.2 mm, resulting in a high ratio of 172.46 of the coupling strength coefficient to the scattering loss coefficient in the fabricated PbP FBG, which exhibits very high reflectivity of 99.99% (i.e., a strong Bragg resonance attenuation of 46.65 dB) and low insertion loss of 0.27 dB. Such high-quality FBGs will be promising in many applications, such as optical fiber communications, sensors, and lasers.

Slit Beam Shaping for Femtosecond Laser Point-by- Point Inscription of High-Quality Fiber Bragg Gratings

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