Abstract: This paper presents a parametric effect, microstructure, micro-hardness and optimization of laser scanning parameters (LSP) on heating experiments during laser assisted machining of Inconel 718 alloy. The laser source used for experiments is a continuous wave Nd:YAG laser with maximum power of 2 kW. The experimental parameters in the present study are cutting speed in the range of 50–100 m/min, feed rate of 0.05–0.1 mm/rev, laser power of 1.25–1.75 kW and approach angle of 60–90°of laser beam axis to tool. The plan of experiments are based on central composite rotatable design L31 (43) orthogonal array. The surface temperature is measured via on-line measurement using infrared pyrometer. Parametric significance on surface temperature is analysed using response surface methodology (RSM), analysis of variance (ANOVA) and 3D surface graphs. The structural change of the material surface is observed using optical microscope and quantitative measurement of heat affected depth that are analysed by Vicker's hardness test. The results indicate that the laser power and approach angle are the most significant parameters to affect the surface temperature. The optimum ranges of laser power and approach angle was identified as 1.25–1.5 kW and 60–65° using overlaid contour plot. The developed second order regression model is found to be in good agreement with experimental values with R2 values of 0.96 and 0.94 respectively for surface temperature and heat affected depth.

Abstract: An emission spectrometer (450-850 nm) using a high-throughput, high numerical aperture (N.A. = 0.3) prism spectrograph with stepped fiberoptic coupling, 32 fast photomultipliers and thirty-two 1.25 GHz digitizers is described. The spectrometer can capture single-shot events with a high dynamic range in amplitude and time (nanoseconds to milliseconds or longer). Methods to calibrate the spectrometer and verify its performance and accuracy are described. When a reference thermal source is used for calibration, the spectrometer can function as a fast optical pyrometer. Applications of the spectrometer are illustrated by using it to capture single-shot emission transients from energetic materials or reactive materials initiated by km⋅s-1 impacts with laser-driven flyer plates. A log (time) data analysis method is used to visualize multiple kinetic processes resulting from impact initiation of HMX (octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine) or a Zr/CuO nanolaminate thermite. Using a gray body algorithm to interpret the spectral radiance from shocked HMX, a time history of temperature and emissivity was obtained, which could be used to investigate HMX hot spot dynamics. Finally, two examples are presented showing how the spectrometer can avoid temperature determination errors in systems where thermal emission is accompanied by atomic or molecular emission lines.

Abstract: Due to lack of reliable thermal diffusivity data of sintered steels in literature, experimental investigations were conducted on samples made of different powder types (based on prealloyed, or diffusion-bonded, or admixed powders) and under different process conditions. So the influence of pressing pressure and sintering temperature on thermal diffusivity was established. Thermal diffusivity was measured using the “flash method”: a sample in the shape of a slab is irradiated with a light pulse on one of the two surfaces, and temperature of the other surface is detected by an ambient temperature pyrometer. The value of the thermal diffusivity is obtained by a least squares regression on the entire trend of the temperature vs. time using the analytical solution of the heat conduction as regression model. Results show the increase of the thermal diffusivity with increasing density. This outcome can be explained from the mutual effect of thermal conductivity and density on thermal diffusivity in porous media. The experimental results have also permitted to verify the influence of the composition of the sintered materials and carbon contents on thermal diffusivity.

Abstract: Experiments in high-energy-density physics often use optical pyrometry to determine temperatures of dynamically compressed materials. In combination with simultaneous shock-velocity and optical-reflectivity measurements using velocity interferometry, these experiments provide accurate equation-of-state data at extreme pressures (P > 1 Mbar) and temperatures (T > 0.5 eV). This paper reports on the absolute calibration of the streaked optical pyrometer (SOP) at the Omega Laser Facility. The wavelength-dependent system response was determined by measuring the optical emission from a National Institute of Standards and Technology-traceable tungsten-filament lamp through various narrowband (40-nm-wide) filters. The integrated signal over the SOP's ∼250-nm operating range is then related to that of a blackbody radiator using the calibrated response. We present a simple closed-form equation for the brightness temperature as a function of streak-camera signal derived from this calibration. Error estimates indicate that brightness temperature can be inferred to a precision of <5%.

Abstract: In order to realize rapid and real temperature measurement for high temperature targets by multi-wavelength pyrometer (MWP), emissivity range constraints to optimize data processing algorithm without effect from emissivity has been developed. Through exploring the relation between emissivity deviation and true temperature by fitting of large number of data from different emissivity distribution target models, the effective search range of emissivity for every time iteration is obtained, so data processing time is greatly reduced. Simulation and experimental results indicate that calculation time is less by 0.2 seconds with 25K absolute error at 1800K true temperature, and the efficiency is improved by more than 90% compared with the previous algorithm. The method has advantages of simplicity, rapidity, and suitability for in-line high temperature measurement.

Abstract: In this work an experimental technique to simultaneously measure the full-field temperature and deformation of composite material subjected to flame heating at high temperature is developed using the technique of image processing. The testing stage is integrated with an oxy-propane flame torch for flame heating, a CCD camera for image recording, a synchronized blue light source for light compensation and an infrared pyrometer for temperature calibration and comparison. The principle of the synchronous measurement of temperature and deformation field is demonstrated and discussed. Experiment on carbon fiber reinforced silicon carbide (C/SiC) composite was conducted to validate this method. The temperature was calculated using an improved two-color method while the displacement field and strain field were calculated using the digital image processing method. Results show that the proposed method is applicable for synchronous measurement of temperature and displacement by using one camera, and the mutual interference between the radiation and reflected light can also be effectively eliminated.

Abstract: A 4-color imaging pyrometer was developed to investigate the thermal behavior of laser-based metal processes, specifically laser welding and laser additive manufacturing of stainless steel. The new instrument, coined a 2x pyrometer, consists of four, high-sensitivity silicon CMOS cameras configured as two independent 2-color pyrometers combined in a common hardware assembly. This coupling of pyrometers permitted low and high temperature regions to be targeted within the silicon response curve, thereby broadening the useable temperature range of the instrument. Also, by utilizing the high dynamic range features of the CMOS cameras, the response gap between the two wavelength bands can be bridged. Together these hardware and software enhancements are predicted to expand the real-time (60 fps) temperature response of the 2x pyrometer from 600 °C to 3500 °C. Initial results from a calibrated tungsten lamp confirm this increased response, thus making it attractive for measuring absolute temperatures of steel forming processes.

Abstract: A newly adapted temperature measurement technique is presented for measuring aerospace relevant high surface temperatures. A comparatively cheap, available digital single-lens reflex camera is used as the imaging system for a two-color ratio pyrometry technique. This provides a highly spatially resolved imaging system that uses the blue, green, and red pixels for the ratio pyrometry measurements. At the Centre for Hypersonics at the University of Queensland, a Canon EOS 400D camera was spectrally calibrated using a tungsten filament lamp and a monochromator. With the knowledge of the spectral response of the pixels, emission ratio calculations determining the temperature can be undertaken for images of any surface, which fulfills the requirement of radiating as a gray body. For this particular camera, the measurable temperature limits were determined to be between approximately 1500 and 3000 K. Two tests cases are presented demonstrating the use of this technique: first, a heated carbon–carbon sample test...

Abstract: In the present work, we propose a new method for measuring the distribution of temperature in the ensembles of condensed-phase particles in plasma spray flows. Interrelation between the spectral temperature of the particles and the distribution of camera brightness signal is revealed. The established inter-relation enables an in-situ calibration of measuring instruments using the objects under study. The spectral-brightness pyrometry method was approbated on a Plazer plasma-arc wire spraying facility at the Paton Institute of Electrical Welding (Ukrainian Academy of Sciences, Kiev) and on the Thermoplasma 50-1 powder spraying facility at the Institute of Theoretical and Applied Mechanics (Russian Academy of Sciences, Siberian Branch, Novosibirsk). The work was supported by the Russian Foundation for Basic Research (Grants Nos. 14-08-90428 and 15-48-00100).

Abstract: Temperature Measurement Using Infrared Spectral Band Emissions From H2O Daniel Jared Ellis Department of Mechanical Engineering, BYU Master of Science Currently there is no known method for accurately measuring the temperature of the gas phase of combustion products within a solid fuel flame The industry standard is a suction pyrometer and thermocouple which is intrusive, both spatially and temporally averaging, and difficult to use In this work a new method utilizing the spectral emission from water vapor is investigated through modeling and experimental measurements This method was demonstrated along a 075m line of sight, averaged over 1 minute in the products of a natural gas flame but has the potential to produce a spatial resolution on the order of 5 cm and a temporal resolution of less than 1 millisecond The method employs the collection of infrared emission from water vapor over discrete wavelength bands and then uses the ratio of those emissions to infer temperature A 125 mm lens has been positioned within a water cooled probe to focus flame product gas emission into an optical fiber where the light is transmitted to a Fourier Transform Infrared Spectrometer (FTIR) The same optical setup was also used to collect light from a black body cavity at a known temperature in order to calibrate the spectral sensitivity of the optical system and FTIR detector Experiments were conducted in the product gas of a 150 kWth methane flame comparing the optical emission results to a suction pyrometer with type K thermocouple The optical measurement produced gas temperatures approximately 1 4% higher than the suction pyrometer Broadband background emission was also seen by the optical measurement and was removed assuming grey body radiation This background emission can be used to determine particle emission temperature and intensity Additional work will be needed to demonstrate the method under conditions with significant particle emission Additional work is also needed to demonstrate the work over a smaller path length and shorter time scale

Abstract: Thermal shocks are applied to a 304L austenitic stainless steel plate with a pulsed laser. A stroboscopic reconstruction is used for infrared (IR) and visible light camera measurements. The displacement fields are measured with a digital image correlation (DIC) technique. Different IR devices are used to measure the temperature variations (i.e. medium wave camera and short wave pyrometry). Several ways of determining the emissivity or absorptivity are discussed. The complete 3D thermal loading is numerically determined by minimising the difference between experimental measurements and finite element analyses of thermal fields. An elastoplastic model is then used to compute mechanical fields that are compared with DIC measurements.

Abstract: A streaked pyrometer has been designed to measure the temperature of ≈100 μm diameter heated targets in the warm dense matter region. The diagnostic has picosecond time resolution. Spatial resolution is limited by the streak camera to 4 μm in one dimension; the imaging system has superior resolution of 1 μm. High light collection efficiency means that the diagnostic can transmit a measurable quantity of thermal emission at temperatures as low as 1 eV to the detector. This is achieved through the use of an f/1.4 objective, and a minimum number of reflecting and refracting surfaces to relay the image over 8 m with no vignetting over a 0.4 mm field of view with 12.5× magnification. All the system optics are highly corrected, to allow imaging with minimal aberrations over a broad spectral range. The detector is a highly sensitive Axis Photonique streak camera with a P820PSU streak tube. For the first time, two of these cameras have been absolutely calibrated at 1 ns and 2 ns sweep speeds under full operational conditions and over 8 spectral bands between 425 nm and 650 nm using a high-stability picosecond white light source. Over this range the cameras had a response which varied between 47 ± 8 and 14 ± 4 photons/count. The calibration of the optical imaging system makes absolute temperature measurements possible. Color temperature measurements are also possible due to the wide spectral range over which the system is calibrated; two different spectral bands can be imaged onto different parts of the photocathode of the same streak camera.

Abstract: Chip-based microheaters have been widely used in many applications, including gas sensors, flow meters, mass sensors, and polymerase chain reaction chambers, where accurate monitoring of temperature is critical The temperature measurement is conventionally done with the aid of a separate sensor, which may add to the cost and inaccuracy In this paper, a built-in temperature sensing method is provided for the microheaters The resistor-based microheater relies on Joule heating mechanism and its resistance is dependent upon its own body temperature, implying that the microheater has an inherent temperature sensing mechanism It is found that an intermittent temperature sampling in the middle of the heating cycle does not disturb the body temperature if the temperature sampling voltage and pulsewidth are sufficiently low and short, respectively The built-in temperature sensing is attributed to the electrical time constant being few orders of magnitude smaller than the thermal time constant The temperature estimation results using the built-in method show excellent agreement with the benchmark measurements from an infrared pyrometer

Abstract: Aluminized propellants produce molten particulates of variable size and temperature. In this work, sizes and three-dimensional positions are determined using digital in-line holography with a pulsed laser. Simultaneously, particle temperatures are measured using two-color pyrometry.

Abstract: The accurate hydrodynamic description of an event or system that addresses the equations of state, phase transitions, dissociations, ionizations, and compressions, determines how materials respond to a wide range of physical environments. To understand dense matter behavior in extreme conditions requires the continual development of diagnostic methods for accurate measurements of the physical parameters. Here, we present a comprehensive diagnostic technique that comprises optical pyrometry, velocity interferometry, and time-resolved spectroscopy. This technique was applied to shock compression experiments of dense gaseous deuterium–helium mixtures driven via a two-stage light gas gun. The advantage of this approach lies in providing measurements of multiple physical parameters in a single experiment, such as light radiation histories, particle velocity profiles, and time-resolved spectra, which enables simultaneous measurements of shock velocity, particle velocity, pressure, density, and temperature and e...

Abstract: Author(s): Valdes, Raymond | Advisor(s): Bennett, Ted D | Abstract: The characterization of thermal barrier coating (TBC) systems is increasingly important because they enable gas turbine engines to operate at high temperatures and efficiency. Phase of photothermal emission analysis (PopTea) has been developed to analyze the thermal behavior of the ceramic top-coat of TBCs, as a nondestructive and noncontact method for measuring thermal diffusivity and thermal conductivity. Most TBC allocations are on actively-cooled high temperature turbine blades, which makes it difficult to precisely model heat transfer in the metallic subsystem. This reduces the ability of rote thermal modeling to reflect the actual physical conditions of the system and can lead to higher uncertainty in measured thermal properties. This dissertation investigates fundamental issues underpinning robust thermal property measurements that are adaptive to non-specific, complex, and evolving system characteristics using the PopTea method. A generic and adaptive subsystem PopTea thermal model was developed to account for complex geometry beyond a well-defined coating and substrate system. Without a priori knowledge of the subsystem characteristics, two different measurement techniques were implemented using the subsystem model. In the first technique, the properties of the subsystem were resolved as part of the PopTea parameter estimation algorithm; and, the second technique independently resolved the subsystem properties using a differential “bare” subsystem. The confidence in thermal properties measured using the generic subsystem model is similar to that from a standard PopTea measurement on a “well-defined” TBC system.Non-systematic bias-error on experimental observations in PopTea measurements due to generic thermal model discrepancies was also mitigated using a regression-based sensitivity analysis. The sensitivity analysis reported measurement uncertainty and was developed into a data reduction method to filter out these “erroneous” observations. It was found that the adverse impact of bias-error can be greatly reduced, leaving measurement observations with only random Gaussian noise in PopTea thermal property measurements.Quantifying the influence of the coating-substrate interface in PopTea measurements is important to resolving the thermal conductivity of the coating. However, the reduced significance of this interface in thicker coating systems can give rise to large uncertainties in thermal conductivity measurements. A first step towards improving PopTea measurements for such circumstances has been taken by implementing absolute temperature measurements using harmonically-sustained two-color pyrometry. Although promising, even small uncertainties in thermal emission observations were found to lead to significant noise in temperature measurements. However, PopTea analysis on bulk graphite samples were able to resolve its thermal conductivity to the expected literature values.