Journal Article10.1107/S0021889809002222
Irena: tool suite for modeling and analysis of small-angle scattering
Jan Ilavsky,Pete R. Jemian +1 more
1.2K
TL;DR: Irena as mentioned in this paper is a tool suite for analysis of both X-ray and neutron small-angle scattering (SAS) data within the commercial Igor Pro application, bringing together a comprehensive suite of tools useful for investigations in materials science, physics, chemistry, polymer science and other fields.
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Abstract: Irena, a tool suite for analysis of both X-ray and neutron small-angle scattering (SAS) data within the commercial Igor Pro application, brings together a comprehensive suite of tools useful for investigations in materials science, physics, chemistry, polymer science and other fields. In addition to Guinier and Porod fits, the suite combines a variety of advanced SAS data evaluation tools for the modeling of size distribution in the dilute limit using maximum entropy and other methods, dilute limit small-angle scattering from multiple non-interacting populations of scatterers, the pair-distance distribution function, a unified fit, the Debye–Bueche model, the reflectivity (X-ray and neutron) using Parratt's formalism, and small-angle diffraction. There are also a number of support tools, such as a data import/export tool supporting a broad sampling of common data formats, a data modification tool, a presentation-quality graphics tool optimized for small-angle scattering data, and a neutron and X-ray scattering contrast calculator. These tools are brought together into one suite with consistent interfaces and functionality. The suite allows robust automated note recording and saving of parameters during export.
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Citations
Quantitative analysis of the morphology of {101} and {001} faceted anatase TiO2 nanocrystals and its implication on photocatalytic activity
Jue Liu,Daniel Olds,Rui Peng,Lei Yu,Guo Shiou Foo,Shuo Qian,Jong Keum,Beth S. Guiton,Zili Wu,Katharine Page +9 more
TL;DR: In this paper, the average morphology and atomistic structure of faceted anatase TiO2 nanocrystals based on differential evolution refinements using Debye scattering equation calculations were obtained.
66
Fibrinogen species as resolved by HPLC-SAXS data processing within the UltraScan Solution Modeler (US-SOMO) enhanced SAS module
Emre H. Brookes,Javier Pérez,Barbara Cardinali,Aldo Profumo,Patrice Vachette,Patrice Vachette,Mattia Rocco +6 more
TL;DR: The usefulness of a new high-performance liquid chromatography/small-angle X-ray scattering (HPLC-SAXS) data analysis module within the multi-resolution modeling suite US-SOMO is illustrated with size-exclusion small-angle SXS data of a crude bovine serum albumin sample.
Nanoporous Iridium Nanosheets for Polymer Electrolyte Membrane Electrolysis
Swarnendu Chatterjee,Xiong Peng,Saad Intikhab,Guosong Zeng,Nancy Kariuki,Deborah J. Myers,Nemanja Danilovic,Joshua Snyder +7 more
Abstract: The growth of the hydrogen economy is predicated on advancements in electrochemical energy technologies, with water electrolysis as a key component to the technological portfolio. Much of the focus on anode catalyst development for polymer electrolyte membrane water electrolyzers (PEMWE) is centered on activity as controlled by compositional and morphological impacts on reactant/intermediate/product adsorption. However, the effectiveness of this strategy is found to be limited upon integration of these materials into PEMWE membrane electrode assemblies (MEA). Regardless of catalyst activity, the combination of electrode inhomogeneity, ionomer integration, and high density of oxide–oxide interfaces yields significant performance losses associated with poor catalytic electrode conductivity. Here many of these limitations are addressed through the development of a unique catalyst morphology composed of nanoporous Ir nanosheets (npIrx‐NS) that exhibit high catalytic activity for the anodic oxygen evolution reaction and superior electrode electronic conductivity in comparison to a commercial IrO2 nanoparticle catalyst. The utility of the npIrx‐NS is demonstrated through incorporation into PEMWE MEAs where their performance exceeds that of commercial catalyst coated membranes at loadings as low as 0.06 mgIr cm−2 while exhibiting a negligible loss in performance following 50 000 accelerated stress test cycles.
65
Collagen Fibril Diameter and Leather Strength
Hannah C. Wells,Richard L. Edmonds,Nigel Kirby,Adrian Hawley,Stephen T. Mudie,Richard G. Haverkamp +5 more
TL;DR: It is suggested that there may be a different structural motif in skin compared with tendon, particularly ovine skin or leather, in which the diameter of the individual fibrils contributes less to strength than fibril alignment does.
65
Inexpensive thermochemical energy storage utilising additive enhanced limestone
TL;DR: In this paper, a thermal energy storage device based on CaCO3 was proposed for a range of applications, e.g. concentrated solar power plants, wind farms, photovoltaics, and excess grid energy.
64
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