Patent
Gas-phase fluorination catalyst and preparation method thereof
Mengfei Luo,Lin Qian,He Jun,Jiqing Lu,Guanqun Xie,Liyang Zhou,Kefeng Chen,Xueliang Zhang +7 more
- 19 Aug 2009
4
TL;DR: In this article, a gas phase fluorination catalyst with high activity and stability and a method for preparing the same so as to overcome the defects of poor activity, stability and robustness existing in the prior gas phase catalysts is presented.
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Abstract: The invention provides a gas phase fluorination catalyst and a method for preparing the same. The aim of the invention is to provide a gas phase fluorination catalyst with high activity and stability and a method for preparing the same so as to overcome the defects of poor activity and stability existing in the prior gas phase fluorination catalyst. The catalyst of the invention comprises a carrier and active components, wherein the carrier is a compound of Y, and the active components comprise a compound of chromium and one or more of compounds of magnesium, aluminum, indium, gallium and zinc. The method for preparing the catalyst comprises: according to a certain ratio, the compounds of Y and Cr and one or more of compounds of magnesium, aluminum, indium, gallium and zinc are weighed up, added with water, evenly mixed and added with a precipitator until the precipitation is finished, and the precipitate is separated and the solution washed until the filtrate is neutral, the precipitate is dried, formed and roasted to give the a precursor of the fluorination catalyst, and the precursor of the fluorination catalyst is added with anhydrous HF and treated at a certain temperature to give the gas phase fluorination catalyst.
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Citations
Patent
Co-production method for 2,3,3,3-tetrafluoropropylene and trans-1,3,3,3-tetrafluoropropylene
Hong Jiangyong,Yang Bo,Ou Yanghao,Zhang Yan,Zhao Yang +4 more
- 23 Feb 2018
TL;DR: In this paper, a co-production method for 2,3, 3, 3-tetrafluoropropylene and trans-1, 3 3-3-3,3-trimethylpolyethylene (TBP) is presented.
1
Patent
Method for preparing fluorinated catalyst by homogeneous precipitation method
Wang Wei,Ding Chen,Xu Qiang,Sun Sen,Zhang Xingquan,Du Rongli +5 more
- 24 Feb 2016
TL;DR: In this paper, a method for preparing a fluorinated catalyst by a homogeneous precipitation method is described, which consists of the steps: taking a solution of a chloride or nitrate of chromium as a main raw material, and adding an alkaline metal chloride or Nitrate; taking urea as a precipitating agent, and constantly stirring and mixing evenly; at the temperature of 85-100 DEG C, carrying out a heat preservation reaction for 2-8 hours, regulating a pH of the solution to be 7.0-8.5, and placing the dried