Journal Article10.1524/ZKRI.2010.1202
Collecting 3D electron diffraction data by the rotation method
TL;DR: In this article, a new method for collecting complete three-dimensional electron diffraction data is described, which is collected by combining electron beam tilt at many very small steps, with rotation of the crystal in a few but large steps.
read more
Abstract: A new method for collecting complete three-dimensional electron diffraction data is described. Diffraction data is collected by combining electron beam tilt at many very small steps, with rotation of the crystal in a few but large steps. A number of practical considerations are discussed, as well as advantages and disadvantages compared to other methods of collecting electron diffraction data.
read more
Chat with Paper
AI Agents for this Paper
Find similar papers on Google Scholar, PubMed and Arxiv
Write a critical review of this paper
Analyze citations of this paper to find unaddressed research gaps
Citations
Chemistry of Covalent Organic Frameworks
TL;DR: Since the organic constituents of COFs, when linked, do not undergo significant change in their overall geometry, it has been possible to predict the structures of the resulting COF, and this advantage has facilitated their characterization using powder X-ray diffraction techniques, which has allowed for the synthesis of COF structures by design and for their formation with the desired composition, pore size, and aperture.
1.5K
Single-Crystal Structure of a Covalent Organic Framework
Yue-Biao Zhang,Jie Su,Hiroyasu Furukawa,Yifeng Yun,Felipe Gándara,Adam Duong,Xiaodong Zou,Omar M. Yaghi +7 more
TL;DR: The crystal structure of a new covalent organic framework, termed COF-320, is determined by single-crystal 3D electron Diffraction using the rotation electron diffraction (RED) method for data collection.
3D Electron Diffraction: The Nanocrystallography Revolution.
Mauro Gemmi,Enrico Mugnaioli,Tatiana E. Gorelik,Ute Kolb,Ute Kolb,Lukáš Palatinus,Philippe Boullay,Sven Hovmöller,Jan Pieter Abrahams,Jan Pieter Abrahams,Jan Pieter Abrahams +10 more
TL;DR: This Outlook reviews most important 3D electron diffraction applications for different kinds of samples and problematics, related with both materials and life sciences.
412
Three-dimensional rotation electron diffraction : software RED for automated data collection and data processing
TL;DR: Implementation of the RED software package for automated collection and processing of rotation electron diffraction data is described.
References
A short history of SHELX
TL;DR: This paper could serve as a general literature citation when one or more of the open-source SH ELX programs (and the Bruker AXS version SHELXTL) are employed in the course of a crystal-structure determination.
Three-dimensional model of purple membrane obtained by electron microscopy
Richard Henderson,P. N. T. Unwin +1 more
TL;DR: A 7-Å resolution map of the purple membrane has been obtained by electron microscopy of tilted, unstained specimens and shows that Lipid bilayer regions fill the spaces between the protein molecules.
2.3K
Double conical beam-rocking system for measurement of integrated electron diffraction intensities
R. Vincent,Paul A. Midgley +1 more
TL;DR: In this article, a double conical scanning system was designed to collect a large data set of integrated intensities that were more suitable for structure determination by electron diffraction, both by removing excitation errors due to curvature of the Ewald sphere and also by reducing non-systematic dynamical effects.
718
Towards automated diffraction tomography: part I--data acquisition.
TL;DR: An experimental software module has been developed for the Tecnai microscope for such an automated diffraction pattern collection while tilting around the goniometer axis that allows automated recording of diffraction tilt series from nanoparticles with a size down to 5nm.
510
•Book
Structure Analysis by Electron Diffraction
B. K. Vaĭnshteĭn,E. Feigl,J. A. Spink +2 more
- 01 Jan 1964
366