The invention relates to a solid super-structure microsphere (Fe3O4@C) wave-absorbing material and a preparation method and application thereof. The method comprises the following steps: preparing a Fe3O4 nanoparticle precursor, preparing Fe3O4 nanoparticles, preparing a microemulsion system, and preparing the Fe3O4@C superstructure microsphere wave-absorbing material. The method is simple, convenient, easy to operate, low in carbonization temperature and low in energy consumption. The prepared Fe3O4@C superstructure microsphere wave-absorbing material has good wave-absorbing efficiency and awide effective absorption frequency band, and can realize effective absorption of full coverage of an X wave band.

Solid Fe3O4@C superstructure microsphere wave-absorbing material and preparation method and application thereof

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Solid Fe3O4@C superstructure microsphere wave-absorbing material and preparation method and application thereof