The JAXA Hayabusa 2 mission returned 5.4 g of material from the C-type asteroid Ryugu. The Mn-Cr ages of dolomite in the returned samples indicate that Ryugu's parent body experienced aqueous alteration sometimes between <1.8 and 6.8 Myr after CAI formation. Because this time range overlaps with the lifetime of the solar nebula, we investigate the possibility that magnetite and pyrrhotite, which are aqueous alteration products found in Ryugu samples, acquired a remanent magnetization reflecting the nebula field intensity. We analyze the intrinsic magnetic properties and paleomagnetic record of three Ryugu samples of 0.82, 0.97 and 21.87 mg. None of the samples exhibit a stable natural remanent magnetization. This indicates that the aqueous alteration of Ryugu's parent body took place either in a field of a few µT, or in a very weak to null field. In the former scenario, the solar nebula field is the most likely magnetizing field, implying that aqueous alteration occurred before its dissipation, i.e., before ∼5 Myr after CAI formation. In the latter scenario, aqueous alteration must have occurred either after the dissipation of the nebula, or at an earlier epoch and a large heliocentric distance (> 5 au). The similarities between Ryugu samples and CI chondrites favor this second hypothesis. Our results contrast with another paleomagnetic study of two Ryugu samples, arguing for a paleofield intensity of 40 to 390 µT. Our interpretation of this discrepancy is that these samples were exposed to artificial magnetic fields (> mT) during preceding experiments. This highlights the importance of conducting, as much as possible, the paleomagnetic investigations of returned samples before any other experiment. We also demonstrate that the ratio of NRM over low-field magnetic susceptibility is a powerful, non-destructive indicator of magnetic contamination. We recommend measuring this ratio routinely before paleomagnetic investigations of meteorites and returned samples. 

Hayabusa 2 returned samples reveal a weak to null magnetic field during aqueous alteration of Ryugu's parent body

Abstract Developing a cleanroom and clean chambers (CCs) for Hayabusa2 returned samples has been discussed with the committee for Hayabusa2 sample curation facility since 2015. One major difference from the specifications of the CCs used for Itokawa samples is that a part of samples was decided to be handled and preserved in vacuum to avoid terrestrial nitrogen contamination with organics or unknown materials that might easily react with the samples. Thus, the CCs for Hayabusa2 samples were divided into two CCs for vacuum processes and three CCs for purified nitrogen conditions. The cleanroom was built in summer 2017, while the CCs were installed in the summer of 2018. After the installation of the CCs, instruments for initial descriptions, sample containers, handling tools for powder and particle samples, and jigs to assist handling samples were developed in parallel with functional checks and repeated rehearsals between the fall of 2018 and the fall of 2020. The curatorial works on Hayabusa2-retuned samples were conducted as previously planned. Simultaneously, contaminations and influences of inorganics, organics, microbial, and magnetic constructs have been assessed to evaluate their potential effects on the analysis of the returned samples. Additionally, the tools used to touch samples directly have been demagnetized to avoid sample magnetization during their handling and the tool magnetization was measured before and after their usages. The series of developments and experiences from the curatorial works of Hayabusa2-returned samples represent valuable implications for future sample return missions. Graphical Abstract 

A curation for uncontaminated Hayabusa2-returned samples in the extraterrestrial curation center of JAXA: from the beginning to present day

Abstract The Hayabusa2 mission provided a unique data set of asteroid Ryugu that covers a wide range of spatial scale from the orbiter remote sensing instruments to the returned samples. The MASCOT lander that was delivered onto the surface of Ryugu aimed to provide context for these data sets by producing in situ data collected by a camera (MasCam), a radiometer (MARA), a magnetometer (MasMag) and a spectrometer (MicrOmega). In this work, we evaluate the success of MASCOT as an integrated lander to bridge the gap between orbiter and returned sample analysis. We find that MASCOT’s measurements and derivatives thereof, including the rock morphology, colour in the visible wavelengths, possible meteorite analogue, density, and porosity of the rock at the landing site are in good agreement with those of the orbiter and the returned samples. However, it also provides information on the spatial scale (sub-millimetres to centimetres) at which some physical properties such as the thermal inertia and reflectance undergo scale-dependent changes. Some of the in situ observations such as the presence of clast/inclusions in rocks and the absence of fine particles at the landing site was uniquely identified by MASCOT. Thus, we conclude that the delivery of an in situ instrument like MASCOT provides a valuable data set that complements and provides context for remote sensing and returned sample analyses. Graphical Abstract 

/pdf/mascots-in-situ-analysis-of-asteroid-ryugu-in-the-context-of-vknu01bl.pdf

MASCOT’s in situ analysis of asteroid Ryugu in the context of regolith samples and remote sensing data returned by Hayabusa2

Visualization of nanoscale magnetic domain states in the asteroid Ryugu

Abstract Single silicate crystals hosting tiny magnetic inclusions are remarkable targets to study the paleointensities of the Earth and extraterrestrial samples. Since the pioneering work done in late 1990s, paleointensity studies using various silicate minerals such as feldspar, quartz, zircon, pyroxene, and olivine with magnetic inclusions trapped during grain growth or exsolved from the host phase have been reported. It has been shown that some single crystals have the ability to record paleomagnetic information as reliable or more reliable than the whole rock, by direct comparison of the obtained paleointensity estimate from single crystal and the whole-rock sample or the magnetic observatory data. Various rock-magnetic studies also support the fidelity of these crystals. Here, we provide a brief review of the rock-magnetic characteristics of the single crystals, the mineralogical background of the hosting silicates, and experimental procedures developed to obtain reliable data from magnetically weak samples with distinctive rock-magnetic features. We also overview the studies on paleointensity and related topics on various terrestrial and extraterrestrial samples published mainly after the comprehensive reviews in late 2000s. The present review covers the advantages as well as the limitations and caveats of paleointensity studies using single crystal samples and will help readers who wish to utilize this technique in their research. Graphical Abstract 

A brief review of single silicate crystal paleointensity: rock-magnetic characteristics, mineralogical backgrounds, methods and applications

In this study, systematic rock magnetic measurements and saturation isothermal remanent magnetization (SIRM) paleointensity calibration experiments were conducted for the returned samples from C‐type asteroid (162173) Ryugu and two carbonaceous chondrites (Orgueil and Tagish Lake) to evaluate the remanence carriers of the Ryugu sample and its ability as a paleomagnetic recorder. Our magnetic measurements show that Ryugu samples exhibit signatures for framboidal magnetite, coarse‐grained magnetite, and pyrrhotite, and that framboidal magnetite is the dominant remanence carrier of Ryugu samples in the middle‐coercivity range. The SIRM paleointensity constant was obtained for two Ryugu samples, and the median value was 3,318 ± 1,038 μT, which is close to the literature's value based on the average among magnetite, titanomagnetite, pyrrhotite, and FeNi alloys and is widely used for SIRM paleointensity experiments. The paleointensity values estimated using the obtained SIRM paleointensity constant indicate a strong magnetic field of the protoplanetary disk, suggesting that Sun's protoplanetary disk existed at the disk location of Ryugu's parent planetesimal when framboidal magnetite precipitated from the aqueous fluid.

Rock Magnetic Characterization of Returned Samples From Asteroid (162173) Ryugu: Implications for Paleomagnetic Interpretation and Paleointensity Estimation

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Rock Magnetic Characterization of Returned Samples From Asteroid (162173) Ryugu: Implications for Paleomagnetic Interpretation and Paleointensity Estimation