Effects of cellulose, hemicellulose, and lignin on the morphology and mechanical properties of metakaolin-based geopolymer

Geopolymers show good potential to be used as free formaldehyde-based binder to produce wood-based panels. Hence, the objective of this research was to investigate the geopolymer composition as binder on the physical and mechanical properties of multi-layered plywood. The geopolymer binder was prepared based on kaolin and metakaolin as the major aluminosilicate powder that were substituted with different contents of silica fume. The results showed that the substitution of aluminosilicate with silica fume (up to 20% based on weight) in the geopolymer mixture modified the chemistry of the geopolymerisation, and hence, improved the amorphous structures of the geopolymer binder. In summary, the substitution of aluminosilicate with silica fume (up to 20% based on weight) in the geopolymer mixture improved the geopolymer binder cohesion, reduced the binder viscosity, reduced the binder curing time, increased the binder penetration into the superficial wood cells, increased the binder shear strength, increased the bending strength of plywood, and accordingly, reduced the plywood stiffness. Notably, none of the plywood samples did delaminate even after 672 h water immersion, implying that the geopolymer binder-based products have a better stability in water compared to some organic binders (e.g., adhesives based on tannin, soya and starch), which suffer from hydrolysis after immersion in water. All in all, the geopolymer binder based on metakaolin showed promising potential to be used as formaldehyde-free binder to produce plywood.

Development of plywood using geopolymer as binder: effect of silica fume on the plywood and binder characteristics

Preparation and properties of geopolymer/soy protein isolate composites by in situ organic-inorganic hybridization: A potential green binder for the wood industry

In this research, a new binder class for wood based composites, named geopolymer binder, was developed based on pozzolanic by-products (e.g. fly ash). Additionally, effects of different amounts of silica fume, as a replacement agent with other aluminosilicate components (e.g. fly ash and metakaolin), have been evaluated in the innovative binder. The Automated Bonding Evaluation System technique was used to characterize the bonding shear strength of the developed geopolymer binder. It was shown that the best shear strength for fly ash based binders was obtained by the lowest press temperature and longest pressing time. The addition of silica fume (from 20% up to 100%) significantly influenced the bonding shear strength in all binder types. Due to the chemical and mineralogical compositions, silica fume displays higher pozzolanic activity than metakaolin whereas fly ash shows lower strength in comparison to metakaolin. The silica fume (100%) based binder has also superior shear strength compared to those of conventional UF resin and other geopolymer binders. Bonding shear strength like that for UF resin was achieved by substituting only 20% silica fume in geopolymer binder compositions.

Effect of aluminosilicate powders on the applicability of innovative geopolymer binders for wood-based composites

CaCl2-induced interfacial deposition for the preparation of high-strength and flame-retardant plywood using geopolymer-based adhesive

Geopolymer binders are an emerging class of mineral polymer that can be manufactured from natural raw materials and industrial byproducts containing high amounts of silica (Si) and alumina (Al) in mineral compositions. Various ratios of materials used for manufacturing geopolymer binder have been tested to evaluate the bonding performance of geopolymers with wood by means of tests performed on an automated bonding evaluation system (ABES). Tests with a binder based on sodium silicate water glass (Na 50T) are partly promising, which resulted only 10% lower shear strength than that based on urea formaldehyde. The binder characteristics were significantly influenced by changing the ratio of SiO2:M2O (M = Na or K) and the ratio solid content to chemical base in the water glass. Expectedly, increasing press temperatures and pressing times showed a positive correlation with the curing performance of geopolymer binder. It was also demonstrated that the binder properties can be changed in wide ranges to obtain binders which fulfill the minimum requirements set by industrial users.

Geopolymers as potential new binder class for the wood based composite industry

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Geopolymers as potential new binder class for the wood based composite industry

Effect of aluminosilicate powders on the applicability of innovative geopolymer binders for wood-based composites