Lanthanide induced shifts and relaxation rate enhancements

Chapter 225 – Rare-earth beta-diketonates

Structures of high coordination complexes

http://www.meilerlab.org/index.php/publications/showPublication/pub_id/100

Expanding the utility of NMR restraints with paramagnetic compounds: background and practical aspects.

Metal chelates of fluorinated 1,3-diketones and related compounds

Lanthanide shift reagents. Survey

Magnetic anisotropy measurements on single crystals of a series of paramagnetic 8-coordinate lanthanide shift reagent adducts of the type Ln[(CH3)3CCOCHCOC(CH3)3(4-CH3C5H1N)2 have been made for the following lanthanides: praseodymium, neodymium, samarium, europium, terbium, dysprosium, holmium, erbium, thulium, and ytterbium. The susceptibility tensors are highly anisotropic and nonaxial. Dipolar nuclear magnetic resonance shifts evaluated from the solid-state date are in satisfactory agreement with the solution results.

https://science.sciencemag.org/content/sci/177/4053/994.full.pdf

Lanthanide complexes as nuclear magnetic resonance structural probes: paramagnetic anisotropy of shift reagent adducts.

Lanthanide shift reagents. X-ray structure of the eight-coordinate bis(4-picoline) adduct of 2,2,6,6-tetramethylheptane-3,5-dionatoholmium, Ho(dpm)3(4-pic)2

Magnetic anisotropy and dipolar shifts in shift reagent systems

Lanthanid-verschiebungsreagentien, roentgenstruktur von achtfach-koordiniertem tris-(2,2,6,6-tetramethyl-heptandion-(3,5)-ato)-holmium-bis-(gamma-picolin)

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