L.) at various angles to the grain. Results show that hardness is highly dependent on grain direction. The hardness value of a radial surface; i.e. when load is applied in tangential direction, is about half of the end–grain surface hardness. For angles between 0 and 90°, hardness measurements are well described by Hankinson's formula. The relation between hardness and density at each load direction has also been studied.

https://link.springer.com/content/pdf/10.1007%2Fs001070050392.pdf

Influence of grain angle on Brinell hardness of Scots pine (Pinus sylvestris L.)

This paper investigates the within- and between-tree variability of hardness and basic den- sity in two stands of 11-year-old and 20-year-old maritime pine trees grown in the south-west of France. A slight increase was found in the inner core hardness of the 11-year-old trees (+13.9 %) and in basic density of the 20-year-old pines (6.5 %) with decreasing tree height. Between the 1st and 13th annual rings of the 20-year-old trees, hardness increased by +49.8 % and basic density by +18.7 % on average. These variations were strongly tree-dependent. A significant correlation was found between hardness and basic density, even when each sampling position was considered indepen- dently. (© Inra/Elsevier, Paris.)

/pdf/hardness-and-basic-density-variation-in-the-juvenile-wood-of-4fst2n95gy.pdf

Hardness and basic density variation in the juvenile wood of maritime pine

A cellular finite element model for the cutting of softwood across the grain

Little is known about historic wood as it ages naturally. Instead, most studies focus on biological decay, as it is often assumed that wood remains otherwise stable with age. This PhD project was organised by Historic Scotland and the University of Glasgow to investigate the natural chemical and physical aging of wood. 
The natural aging of wood was a concern for Historic Scotland as traditional timber replacement is the standard form of repair used in wooden cultural heritage; replacing rotten timber with new timber of the same species. The project was set up to look at what differences could exist both chemically and physically between old and new wood, which could put unforeseen stress on the joint between them. Through Historic Scotland it was possible to work with genuine historic wood from two species, Oak and Scots pine, both from the 1500’s, rather than relying on artificial aging. Artificial aging of wood is still a debated topic, with consideration given to whether it is truly mimicking the aging process or just damaging the wood cells.
The chemical stability of wood was investigated using Fourier-transform infrared (FTIR) microscopy, as well as wet chemistry methods including a test for soluble sugars from the possible breakdown of the wood polymers. The physical properties assessed included using a tensile testing machine to uncover possible differences in mechanical properties. An environmental chamber was used to test the reaction to moisture of wood of different ages, as moisture is the most damaging aspect of the environment to wooden cultural objects. The project uncovered several differences, both physical and chemical, between the modern and historic wood which could affect the success of traditional ‘like for like’ repairs. Both oak and pine lost acetyl groups, over historic time, from their hemicellulose polymers. This chemical reaction releases acetic acid, which had no effect on the historic oak but was associated with reduced stiffness in historic pine, probably due to degradation of the hemicellulose polymers by acid hydrolysis. The stiffness of historic oak and pine was also reduced by decay. Visible pest decay led to loss of wood density but there was evidence that fungal decay, extending beyond what was visible, degraded the S2 layer of the pine cell walls, reducing the stiffness of the wood by depleting the cellulose microfibrils most aligned with the grain. Fungal decay of polysaccharides in pine wood left behind sugars that attracted increased levels of moisture.
 The degradation of essential polymers in the wood structure due to age had different impacts on the two species of wood, and raised questions concerning both the mechanism of aging of wood and the ways in which traditional repairs are implemented, especially in Scots pine. These repairs need to be done with more care and precision, especially in choosing new timber to match the old. Within this project a quantitative method of measuring the microfibril angle (MFA) of wood using polarised Fourier transform infrared (FTIR) microscopy has been developed, allowing the MFA of both new and historic pine to be measured. This provides some of the information needed for a more specific match when selecting replacement timbers for historic buildings.

The structural and mechanical integrity of historic wood

Hardness has been considered an important indicator of wood quality and presents a high correlation with density, and, as far as the authors know, there is no specific methodology to evaluate the hardness of charcoal. In this context, it is necessary to develop a reliable and efficient methodology to classify charcoal mechanical properties. Therefore, the aim of this study was to establish multivariate models to estimate dynamic hardness and density of wood and charcoal based on near-infrared spectra. For this, nine wood specimens were examined and pyrolyzed at 300, 450, 600 and 750 °C. The density of wood and charcoal was determined according to standard NBR 11941 (2003) and hydrostatic method, respectively. Dynamic hardness of wood and charcoal was determined by an automated portable hardness tester. Materials submitted to thermal treatment have different spectral signatures compared to those obtained by the wood. Charcoals produced at temperatures of 450, 600 and 750 °C exhibit similar behaviour, with low absorbance compared to wood and thermally treated material at 300 °C, indicating homogenization of charcoal caused by pyrolysis temperature. NIR spectroscopy was able to estimate density and dynamic hardness of wood and charcoal. Charcoal produced at 450 °C obtained a model with highest coefficient of determination and smaller errors. The results show the potential of NIR technology for fast and reliable estimation of physical and mechanical properties of charcoal based on spectra recorded on charcoal and even from wood before pyrolysis.

Estimating hardness and density of wood and charcoal by near-infrared spectroscopy

The deformation processes involved in wedge indentation of wood are described. The behaviour of wood is compared to that of an elastic-plastic solid and that of a cellular body. It approximates towards the former when its density is high and towards the latter when its density is low. The hardness of wood is examined as a function of density and of wedge angle.

Indentation of wood by wedges

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Indentation of wood by wedges