Strengthening the heat-affected zone in actual weld joint of Inconel 625 alloys was crucial for engineering applications in aerospace, petroleum, nuclear energy, and marine industries. In this study, Gleeble thermal simulations were employed to investigate the influence of welding heat on grain morphology, carbide evolution, and mechanical properties of Inconel 625 alloys manufactured by selective laser melting (SLM). Typical elongated columnar grains along the building direction and parallel columnar array with obvious layer boundaries along the scanning direction were observed in SLM-processed Inconel 625 alloys with hot isostatic processing treatment. After Gleeble thermal simulations, the prominent equiaxed grains appeared in the entire gauge region that was directly exposed to the simulated welding heat owing to the recrystallization process. Meanwhile, the size of equiaxed grains significantly increased with the increasing peak temperature. Particularly, only MC-type carbides were observed in the γ-Ni matrix before and after the thermal simulation owing to the fairly rapid heating (100 °C/s) and cooling (30 °C/s) process. Simulated welding heat produced a negative effect on the mechanical properties of the Inconel 625 alloys, especially for the peak temperature of 1350 °C. Then, the respective contributions of the four conventional strengthening mechanisms were successfully quantified for understanding the effect of the simulated peak temperature on the yield strength of the Inconel 625 alloys. Finally, the observations of microstructural evolution indicated that the cross-slip of dislocations was the dominant deformation mechanism to account for the large strain-hardening rate of the Inconel 625 alloys.

Effect of welding thermal treatment on the microstructure and mechanical properties of nickel-based superalloy fabricated by selective laser melting

Characterization on the gradient microstructure near the fusion interface of dissimilar metal between high Cr heat-resistant steel and Ni-based Alloy 617

Analysis of carbide transformation in MC-M23C6 and its effect on mechanical properties of Ni-based superalloy

The relationship between the microstructure and impact toughness, especially the formation of the lamellar carbides and its effect on the impact toughness of the heat-affected zone of Alloy 617 (Alloy 617-HAZ), was systematically investigated. Impact test was performed on Alloy 617/9%Cr dissimilar welded joints aged for different time at 620 °C. The results showed that the characteristic zones of the whole welded joint revealed decreased impact toughness with increasing the aging time. The impact energies in weld metal showed high stability despite the aging process, while the Alloy 617-HAZ for all testing specimens presented the lowest impact toughness with various aging time. Meanwhile, the mixed grains were found in the base metal (BM) and heat-affected zone of Alloy 617, together with the twins with different widths located in the interior of the large grains. The columnar and equiaxed grain zones appear alternately due to the multilayer and multi-pass welding technique. In particular, compared with Alloy 617-BM, coarsened and even lamellar carbides were observed in Alloy 617-HAZ. These special carbides can separate the grains and therefore result in the formation of intergranular fracture morphology in Alloy 617-HAZ. Besides, the microhardness distribution was tested with a proper load, and the results exhibited that the weld possessed the highest hardness for all specimens with various aging time. The higher microhardness in Alloy 617-HAZ compared with that in Alloy 617-BM was attributed to the high density of the dislocations, which could be detected by transmission electron microscope. As a result, the coarsened carbides aggregated in the grain boundaries to form the lamellar layer are deemed as the main factor to reduce the impact toughness in Alloy 617-HAZ.

Formation of Lamellar Carbides in Alloy 617-HAZ and Their Role in the Impact Toughness of Alloy 617/9%Cr Dissimilar Welded Joint

Precipitation behavior and age hardening effect of the precipitates in a Fe-13Cr-4Al-2Mo-1.2Nb alloy

Evolution of carbides and its characterization in HAZ during NG-TIG welding of Alloy 617B

The evolution behavior of second phases during long-term creep rupture process for modified 9Cr-1.5Mo-1Co steel welded joint

The rupture behavior of the modified 10Cr–1Mo steel multi-layer welded joint is determined by the fine-grain zones of the weld metal adjacent to the fusion line during the long-term creep test at 620 °C. The microstructures of multi-layer weld metal before and after the creep tests were characterized in detail, and its role in creep behavior was systematically investigated. Most grain boundaries of subgrains represented the low-angle boundaries in the weld metal adjacent to the fusion line both before and after the creep test. The widths of grains in the fine-grain zones were about 0.5–1 μm. The fracture morphology appeared as “wave” structure due to the cracking initiating from multi-layer grain boundaries in the fine-grain zones. Some W elements that melted into weld metal adjacent to the fusion line altered the thermodynamic and kinetic conditions of the Laves phase formation during long-term creep exposure. Laves phase particles mainly distributed along the grain boundaries due to the faster diffusion and segregation of Mo, W, and Si elements. Moreover, higher-density grain boundaries in the fine-grain zones led to easier nucleation and growth of Laves phase particles. Compared with other areas in the welded joint, the size of Laves phase particles in the fine-grain zones of the weld metal adjacent to the fusion line was the largest ones. The interface between Laves phase particles and the matrix acted as the nucleation site of creep micro-cavities. The creep micro-cavities grew up at the expense of fine-grain boundaries and even grew across the grain boundary deeply into adjacent grains, and then developed to cracks in the fine-grain zones.

Characterization of Multi-layer Weld Metal and Creep–Rupture Behavior of Modified 10Cr–1Mo Welded Joint

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Evolution of carbides and its characterization in HAZ during NG-TIG welding of Alloy 617B

The evolution behavior of second phases during long-term creep rupture process for modified 9Cr-1.5Mo-1Co steel welded joint

Characterization of Multi-layer Weld Metal and Creep–Rupture Behavior of Modified 10Cr–1Mo Welded Joint