Liquid-infused surfaces (or lubricant-infused surfaces) (LIS) are a new class of functional materials introduced in 2011. Their exceptional properties have earned them a place at the forefront of many fields including anti-biofouling, anti-icing, anti-corrosion, drag reduction, droplet manipulation and drop-wise condensation. Integral to their success is the infused lubricant layer which affords them their properties. In this review, we examine the current state of the literature relating to the lubricant layer. We consider the lubricant through all stages in the surface's lifecycle from design, to use, all the way through to depletion and eventual failure. First, we examine trends in lubricant choice and how to choose a lubricant, including environmental and medical considerations. We then look at the different methods used to infuse lubricant into surfaces and how lubricant depletes from the surface. We then report direct and indirect methods to characterise the thickness and distribution of the lubricant layer. Finally, we examine how droplets interact with LIS and the unique properties afforded by the lubricant before providing an outlook into where research centred on understanding the lubricant layer is heading in the new decade.

Life and death of liquid-infused surfaces: a review on the choice, analysis and fate of the infused liquid layer.

The challenge of lubricant-replenishment on lubricant-impregnated surfaces

The appearance of the first laser approximately 12 years after the invention of holography by Gabor (1948) revolutionized the field of optical metrology. In fact, the invention of holographic interferometry enabled the exploitation of interferometry on non-mirror surfaces and full-scale objects. The holography-based measurement methods has been implemented to several industrial systems or in support of R&D with the aim of improving new products in many fields (automotive, aerospace, electronics, etc.). To date, holography has been considered an important measurement tool for non-destructive inspection (NDI), strain-stress measurement, and vibration analysis at various engineering sites. Recently, the new paradigm of Industry4.0 has seen the introduction of new technologies and methods of processing materials as well as the development of manufacturing approaches for the realization of innovative products. For example, direct printing, additive, and bottom-up manufacturing processes are expected to involve new ways of making products in future, and most innovative fabrication processes will be based on the manipulation of soft matter (e.g., starting from the liquid phase) that will be shaped at the nanoscale. The inherent characteristics of digital holography (DH) make it a powerful and accurate tool for the visualization and testing of final products, as well as for in situ and real-time monitoring and quantitative characterization of the processes involved during the fabrication cycle. This review aims to report on the most useful applications of soft matter, where the capabilities offered by DH, such as three-dimensional (3D) imaging, extended focus, 3D tracking, full-field analysis, high sensitivity, and a wide range of measurements from nanometers to centimeters, permit completely non-invasive characterizations on a full-scale. Several holographic experimental results of typical samples are reported and discussed where DH plays a primary role as a tool gauge for soft matter. ACCEPTED ARTICLE PREVIEW

Digital holography as metrology tool at micro-nanoscale for soft matter

Slippery lubricant-infused surfaces allow easy removal of liquid droplets on surfaces. They consist of textured or porous substrates infiltrated with a chemically compatible lubricant. Capillary forces help to keep the lubricant in place. Slippery surfaces hold promising prospects in applications including drag reduction in pipes or food packages, anticorrosion, anti-biofouling, or anti-icing. However, a critical drawback is that shear forces induced by flow lead to depletion of the lubricant. In this work, a way to overcome the shear-induced lubricant depletion by replenishing the lubricant from the flow of emulsions is presented. The addition of small amounts of positively charged surfactant reduces the charge repulsion between the negatively charged oil droplets contained in the emulsion. Attachment and coalescence of oil droplets from the oil-in-water emulsion at the substrate surface fills the structure with the lubricant. Flow-induced lubrication of textured surfaces can be generalized to a broad range of lubricant-solid combinations using minimal amounts of oil.

https://onlinelibrary.wiley.com/doi/pdf/10.1002/advs.201900019

Flow-Induced Long-Term Stable Slippery Surfaces

Liquid flowing around a solid edge, i.e., overflow, is a commonly observed flow behavior. Recent research into surface wetting properties and microstructure-controlled overflow behavior has attracted much attention. Achieving controllable macroscale liquid dynamics by manipulating the micro-nanoscale liquid overflow has stimulated diverse scientific interest and fostered widespread use in practical applications. In this review, we outline the evolution of overflow and present a critical survey of the mechanism of surface wetting properties and microstructure-controlled liquid overflow in multilength scales ranging from centimeter to micro and even nanoscale. We summarize the latest progress in utilizing the mechanisms to manipulate liquid overflow and achieve macroscale liquid dynamics and in emerging applications to manipulate overflow for sustainable development in various fields, along with challenges and perspectives.

Overflow Control for Sustainable Development by Superwetting Surface with Biomimetic Structure.

Wet and dry foams are prevalent in many industries, ranging from the food processing and commercial cosmetic sectors to industries such as chemical and oil-refining. Uncontrolled foaming results in product losses, equipment downtime or damage and cleanup costs. To speed up defoaming or enable anti-foaming, liquid oil or hydrophobic particles are usually added. However, such additives may need to be later separated and removed for environmental reasons and product quality. Here, we show that passive defoaming or active anti-foaming is possible simply by the interaction of foam with chemically or morphologically modified surfaces, of which the superamphiphobic variant exhibits superior performance. They significantly improve retraction of highly stable wet foams and prevention of growing dry foams, as quantified for beer and aqueous soap solution as model systems. Microscopic imaging reveals that amphiphobic nano-protrusions directly destabilize contacting foam bubbles, which can favorably vent through air gaps warranted by a Cassie wetting state. This mode of interfacial destabilization offers untapped potential for developing efficient, low-power and sustainable foam and froth management. Wong et al. demonstrate the efficacy of super-amphiphobic surfaces for in situ defoaming and inhibition of foam growth while handling aqueous solutions. Without the use of chemical additives, their passive approach suggests a facile alternative route to froth management in industrial processes.

/pdf/super-liquid-repellent-surfaces-for-anti-foaming-and-froth-54rpjxzou9.pdf

Super liquid repellent surfaces for anti-foaming and froth management

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Flow-Induced Long-Term Stable Slippery Surfaces

Super liquid repellent surfaces for anti-foaming and froth management