Flexible transparent electrodes (FTEs) with embedded metal meshes play an indispensable role in many optoelectronic devices due to their excellent mechanical stability and environmental adaptability. However, low‐cost, simple, efficient, and environmental friendly integrated manufacturing of high‐performance embedded metal meshes remains a huge challenge. Here, a facile and novel fabrication method is proposed for FTEs with an embedded metal mesh via liquid substrateelectric‐field‐driven microscale 3D printing process. This direct printing strategy avoids tedious processes and offers low‐cost and high‐volume production, enabling the fabrication of high‐resolution, high‐aspect ratio embedded metal meshes without sacrificing transparency. The final manufactured FTEs with 80 mm × 80 mm embedded metal mesh offers excellent optoelectronic performance with a sheet resistance (Rs) of 6 Ω sq−1 and a transmittance (T) of 85.79%. The embedded metal structure still has excellent mechanical stability and good environmental suitability under different harsh working conditions. The practical feasibility of the FTEs is successfully demonstrated with a thermally driven 4D printing structure and a resistive transparent strain sensor. This method can be used to manufacture large areas with facile, high‐efficiency, low‐cost, and high‐performance FTEs.

https://onlinelibrary.wiley.com/doi/pdfdirect/10.1002/advs.202105331

Directly Printed Embedded Metal Mesh for Flexible Transparent Electrode via Liquid Substrate Electric‐Field‐Driven Jet

The idea of four-dimensional (4D) printing is the formation of intricate stimuli-responsive 3D architectures that transform into different forms and shapes upon exposure to environmental stimuli. 4D printing (4DP) of smart/intelligent materials is a promising and novel approach to generate intricate structures for biomedical, food, electronics, textile, and agricultural fields. Nowadays, soft robotics is a growing research field focusing on developing micro/nanoscale 4D-printed robots using intelligent materials. Herein, recent advancements in 4DP of soft robotics, actuators, and grippers are summarized. This review also highlights some recent developments in novel robotics technologies and materials including multi-material printing, electro-, and magneto-active soft materials (MASMs), and metamaterials. It also sheds light on different modeling mechanisms including numerical models and machine learning (ML) models for fabricating highly precise and efficient micro/macro-scaled robots. The applications of shape-memory polymers (SMPs), hydrogels, and liquid crystal elastomers (LCEs)-based 4D-printed soft and intelligent robots in different engineering fields are highlighted. Lastly, this review incorporates current challenges which are hindering the actual utilization of 4D-printed soft robotics and their possible remedies. 

4D printing: Technological developments in robotics applications

Flexible strain sensors have received widespread attention because of their great potential in many fields. Carbon nanotubes (CNTs) have been used as conductive materials for flexible strain sensors due to their excellent electrical and mechanical properties, and the fabricated flexible strain sensors have excellent sensing performance. This paper systematically summarizes the advances in flexible resistance‐type strain sensors based on CNTs. The strain sensing mechanisms are introduced, including crack extension, tunneling effect, and disconnection of overlapping materials. The performance parameters of the sensors, including sensitivity, stretchability, linearity, hysteresis, dynamic durability, and transparency, are discussed comprehensively. The coating methods, 3D printing techniques, chemical vapor deposition, transfer methods, and spinning processes used to fabricate CNT strain sensors are highlighted. The effect of isolated and porous internal conductive structures, folded and microcracked surface structures, films and fabrics macroscopic structures on sensor performance were systematically analyzed. The applications of the sensors in medical health, motion monitoring, gesture recognition, human–computer interaction, and soft robotics are provided in detail. Finally, the future challenges of CNT flexible strain sensors are summarized and the outlook is presented. Although CNT strain sensors have made great progress so far, there are still many problems that need researchers’ attention and solutions.

Carbon Nanotube‐Based Strain Sensors: Structures, Fabrication, and Applications

Perovskite solar cells (PSCs) are promising photovoltaic (PV) technologies due to their high-power conversion efficiency (PCE) and low fabrication cost. This review article delves into the changing PSC landscape by...

Dimensional Diversity (0D, 1D, 2D, 3D) in Perovskite Solar Cells: Exploring the Potential of Mix-dimensional Integrations

Flexible and stretchable transparent electrodes are widely used in smart display, energy, wearable devices and other fields. Due to the limitations of flexibility and stretchability of indium tin oxide electrodes, alternative electrodes have appeared, such as metal films, metal nanowires, and conductive meshes. However, few of the above electrodes can simultaneously have excellent flexibility, stretchability, and optoelectronic properties. Nanofiber (NF), a continuous ultra-long one-dimensional conductive material, is considered to be one of the ideal materials for high-performance transparent electrodes with excellent properties due to its unique structure. This paper summarizes the important research progress of NF flexible transparent electrodes (FTEs) in recent years from the aspects of NF electrode materials, preparation technology and application. First, the unique advantages and limitations of various NF materials are systematically discussed. Then, we summarize the preparation technology of various advanced NF FTEs, and point out the future development trend. We also discuss the application of NFs in solar cells, supercapacitors, electric heating equipments, sensors, etc, and analyze its development potential in flexible electronic equipment, as well as problems that need to be solved. Finally, the challenges and future development trends are proposed in the wide application of NF FTEs in the field of flexible optoelectronics.

Recent advances in nanofiber-based flexible transparent electrodes

Transparent glass with metal mesh is considered a promising strategy for high performance transparent glass heaters (TGHs). However, the realization of simple, low-cost manufacture of high performance TGHs still faces great challenges. Here, a technique for the fabrication of high performance TGHs is proposed using liquid sacrificial substrate electric-field-driven (LS-EFD) microscale 3D printing of thick film silver paste. The liquid sacrificial substrate not only significantly improves the aspect ratio (AR) of silver mesh, but also plays a positive role in printing stability. The fabricated TGHs with a line width of 35 µm, thickness of 12.3 µm, and pitch of 1000 µm exhibit a desirable optoelectronic performance with sheet resistance (Rs ) of 0.195 Ω sq-1 and transmittance (T) of 88.97%. A successful deicing test showcases the feasibility and practicality of the manufactured TGHs. Moreover, an interface evaporator is developed for the coordination of photothermal and electrothermal systems based on the high performance TGHs. The vapor generation rate of the device reaches 10.69 kg m-2 h-1 with a voltage of 2 V. The proposed technique is a promising strategy for the cost-effective and simple fabrication of high performance TGHs.

3D Printed High Performance Silver Mesh for Transparent Glass Heaters through Liquid Sacrificial Substrate Electric-Field-Driven Jet.

Flexible Transparent Electrodes In article number 2105331, Xiaoyang Zhu, Hongbo Lan, and co‐workers develop a fabrication method for flexible transparent electrodes (FTEs) with embedded metal mesh via liquid substrate electric‐fielddriven microscale 3D printing. This method enables the embedded metal mesh with high resolution and high aspect ratio to be formed directly. Moreover, the fabricated FTEs show good application in intelligent structures and sensors.

Directly Printed Embedded Metal Mesh for Flexible Transparent Electrode via Liquid Substrate Electric‐Field‐Driven Jet (Adv. Sci. 14/2022)

Polycaprolactone (PCL) scaffolds have been widely used in biological manufacturing engineering. With the expansion of the PCL application field, the manufacture of high-resolution complex microstructure PCL scaffolds is becoming a technical challenge. In this paper, a novel PCL high-resolution fused deposition 3D printing based on electric field-driven (EFD) jet deposition is proposed to manufacture PCL porous scaffold structures. The process principle of continuous cone-jet printing mode was analyzed, and an experimental system was constructed based on an electric field driven jet to carry out PCL printing experiments. The experimental studies of PCL-fused deposition under different gas pressures, electric field voltages, motion velocities and deposition heights were carried out. Analysis of the experimental results shows that there is an effective range of deposition height (H) to realize stable jet printing when the applied voltage is constant. Under the stretching of electric field force and viscous drag force (FD) with increasing movement velocities (Vs) at the same voltage and deposition height, the width of deposition lines was also gradually decreased. The width of the deposition line and the velocity of the deposition platform is approximately a quadratic curve. The bending phenomenon of deposition lines also gradually decreases with the increase of the movement velocities. According to the experiment results, a single layer linear grid structure was printed under the appropriate process parameters, with compact structure, uniform size and good straightness. The experimental results verify that the PCL porous scaffold structure can be accurately printed and manufactured.

/pdf/experimental-analysis-of-polycaprolactone-high-resolution-3ftplmhx.pdf

Experimental Analysis of Polycaprolactone High-Resolution Fused Deposition Manufacturing-Based Electric Field-Driven Jet Deposition

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Directly Printed Embedded Metal Mesh for Flexible Transparent Electrode via Liquid Substrate Electric‐Field‐Driven Jet

3D Printed High Performance Silver Mesh for Transparent Glass Heaters through Liquid Sacrificial Substrate Electric-Field-Driven Jet.

Directly Printed Embedded Metal Mesh for Flexible Transparent Electrode via Liquid Substrate Electric‐Field‐Driven Jet (Adv. Sci. 14/2022)

Experimental Analysis of Polycaprolactone High-Resolution Fused Deposition Manufacturing-Based Electric Field-Driven Jet Deposition