Catalysis is essential to modern life and has a huge economic impact. The development of new catalysts critically depends on synthetic methods that enable the preparation of tailored nanomaterials. Pulsed laser in liquids synthesis can produce uniform, multicomponent, nonequilibrium nanomaterials with independently and precisely controlled properties, such as size, composition, morphology, defect density, and atomistic structure within the nanoparticle and at its surface. We cover the fundamentals, unique advantages, challenges, and experimental solutions of this powerful technique and review the state-of-the-art of laser-made electrocatalysts for water oxidation, oxygen reduction, hydrogen evolution, nitrogen reduction, carbon dioxide reduction, and organic oxidations, followed by laser-made nanomaterials for light-driven catalytic processes and heterogeneous catalysis of thermochemical processes. We also highlight laser-synthesized nanomaterials for which proposed catalytic applications exist. This review provides a practical guide to how the catalysis community can capitalize on pulsed laser in liquids synthesis to advance catalyst development, by leveraging the synergies of two fields of intensive research.

Pulsed Laser in Liquids Made Nanomaterials for Catalysis.

0D, 1D and 2D nanomaterials for visible photoelectrochemical water splitting. A Review

Ru/TiO2 catalyst for selective hydrogenation of benzene: Effect of surface hydroxyl groups and spillover hydrogen

Bimetallic Ru–M/TiO2 (M = Fe, Ni, Cu, Co) nanocomposite catalysts facribated by galvanic replacement: Structural elucidation and catalytic behavior in benzene selective hydrogenation

Bimetallic Pd-M (M = Pt, Ni, Cu, Co) nanoparticles catalysts with strong electrostatic metal-support interaction for hydrogenation of toluene and benzene

Effect of support composition on the structural and catalytic properties of Ru/AlOOH–SiO2 catalysts for benzene selective hydrogenation

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Bimetallic Ru–M/TiO2 (M = Fe, Ni, Cu, Co) nanocomposite catalysts facribated by galvanic replacement: Structural elucidation and catalytic behavior in benzene selective hydrogenation

Effect of support composition on the structural and catalytic properties of Ru/AlOOH–SiO2 catalysts for benzene selective hydrogenation