Metal oxides are the key ingredients for the development of many advanced functional materials and smart devices. Nanostructuring has emerged as one of the best tools to unlock their full potential. Tungsten oxides (WOx) are unique materials that have been rigorously studied for their chromism, photocatalysis, and sensing capabilities. However, they exhibit further important properties and functionalities that have received relatively little attention in the past. This Feature Article presents a general review of nanostructured WOx, their properties, methods of synthesis, and a description of how they can be used in unique ways for different applications. Tungsten oxides (WOx) are unique functional materials that can be obtained in a vast variety of nanostructured forms. This Feature Article presents a comprehensive review on the properties of WOx that goes beyond chromism and photocatalysis, for which they are usually investigated for. This is followed by a survey of their synthesis methods and implementations for different applications.

Nanostructured Tungsten Oxide – Properties, Synthesis, and Applications

Electrochromics for smart windows: Oxide-based thin films and devices

Surface-Wave Devices for Signal Processing

A review of some papers published in the last fifty years that focus on the semiconducting metal oxide (SMO) based sensors for the selective and sensitive detection of various environmental pollutants is presented.

/pdf/semiconducting-metal-oxide-based-sensors-for-selective-gas-1vi0rm8g60.pdf

Semiconducting Metal Oxide Based Sensors for Selective Gas Pollutant Detection

Piezoelectric sensing is of increasing interest for high-temperature applications in aerospace, automotive, power plants and material processing due to its low cost, compact sensor size and simple signal conditioning, in comparison with other high-temperature sensing techniques. This paper presented an overview of high-temperature piezoelectric sensing techniques. Firstly, different types of high-temperature piezoelectric single crystals, electrode materials, and their pros and cons are discussed. Secondly, recent work on high-temperature piezoelectric sensors including accelerometer, surface acoustic wave sensor, ultrasound transducer, acoustic emission sensor, gas sensor, and pressure sensor for temperatures up to 1,250 °C were reviewed. Finally, discussions of existing challenges and future work for high-temperature piezoelectric sensing are presented.

/pdf/high-temperature-piezoelectric-sensing-4t4e813w78.pdf

High-Temperature Piezoelectric Sensing

High temperature acoustic wave (AW) devices capable of operating above 600degC and in hostile environments have opened potential applications for monitoring industrial processes, power plants, and aerospace systems. The authors have reported on the development of thin film electrodes and protective ceramic layers to allow surface acoustic wave (SAW) device operation up to 800degC on langasite (LGS) crystals. This success motivated further study of the electrode material and protective ceramic overlayer, as well as investigations of long term performance, temperature cycling and shock behavior, which are reported in this work. Among the results reported are: behavior of a co-deposited Pt/Rh/ZrO2 composite electrode structure up to 1000degC; investigation of oxygen rich and nitrogen rich SiAlON protective ceramic layers; long term (4080 hours, or about 5frac12 months) operation of a two-port SAW resonator at 800degC; cyclical thermal tests between room temperature and 850degC; and thermal shock tests of crystals between 700degC and room temperature.

High temperature stability of langasite surface acoustic wave devices

Structure, conductivity, and optical absorption of Ag2−xO films

Nanostructured tungsten and tungsten trioxide films prepared by glancing angle deposition

Single crystal sapphire wafers with <1 nm root mean square (RMS) roughness are ideal substrates for chemiresistive sensors that utilize ultra-thin (<50 nm thick) semiconducting metal oxide (SMO) films. Platinum metallization on a highly polished sapphire platform to form electrodes, heater, and a resistive temperature device (RTD) requires the use of a very thin (<20 nm) buffer layer, such as Ti or Zr, to achieve good adhesion at the Pt/sapphire interface. Using AES, secondary ion mass spectroscopy (SIMS), XRD, and wire bond tests before and after annealing treatments, we have found that Zr has superior performance as an adhesion layer compared to Ti. At temperatures of 200–700°C, required for RTD and SMO film stabilization as well as prolonged sensor operation, there is significant migration of Ti through the Pt film, whereas the Zr layer is less mobile. The Pt/Zr/sapphire architecture also minimizes delamination failure of wire bonds to the sensor device.

Performance of Zr and Ti adhesion layers for bonding of platinum metallization to sapphire substrates

This paper reviews current progress in the area of wireless microwave acoustic sensor technology, and discusses advances in wireless interrogation systems that can operate in harsh environments. The use of wireless, battery-free, low maintenance surface acoustic wave (SAW) sensors has been successfully demonstrated in applications including high temperature turbine engines and inflatable aerospace structures. Wireless interrogation of multiple sensors up to 910°C has been established and sensor tests in gas turbine engine are reported. This paper elaborates on several aspects of the technology, including: high-temperature thin-film electrode and sensor development, temperature cycling, thermal-shock behavior, testing in turbine engine environments, sensor packaging and attachment, wireless operation, and adaptation to energy and industrial applications.

Wireless acoustic wave sensors and systems for harsh environment applications

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